HuagongsheHuagongshe Chemistry Print Report · For research reference only
Ethanol → HCID 3735222, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Ethanol | HCID 702 | — |
| Reactant | Sodium Hydroxide | HCID 14798 | — |
| Reactant | 4'-(10-Acetyloxydecyloxy)biphenyl-4-carboxylic acid ethyl ester | HCID 53820252 | — |
| Solvent | Water | HCID 962 | — |
| Product | HCID 3735222 | HCID 3735222 | 97.3% |
Reaction Steps
30 m moles (13.2 g) of the above 4'-(10-acetyloxydecyloxy) biphenyl-4-carboxylic acid ethyl ester and 10 g of sodium hydroxide were stirred for 10 min. at 70° C. in a mixed solvent of 40 ml of ethanol and 80 ml of water. After the reaction, the reaction solution was concentrated to obtain 10.8 g of 4'-(10-hydroxydecyloxy)biphenyl-4-carboxylic acid. (yield: 97%)
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US04913839 |
| Source dataset | uspto-grants-1990_04 |
| ORD ID | ord-1d61dd5f42d54ecf82da2f024943d1e6 |
| Source note | uspto-grants-1990_04 |