HuagongsheHuagongshe Chemistry Print Report · For research reference only
2-(Methylamino)ethanol → HCID 14499650, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | 2-(Methylamino)ethanol | HCID 8016 | — |
| Reactant | Potassium Carbonate | HCID 11430 | — |
| Reactant | 1-(Azepan-1-yl)-2-chloroethan-1-one | HCID 3144134 | — |
| Solvent | Methyl Ethyl Ketone | HCID 6569 | — |
| Product | HCID 14499650 | HCID 14499650 | — |
Reaction Steps
A mixture of 4.8 g (27 mmol) of 1-(2-chloroacetyl)perhydroazepine, dissolved in 40 ml of 2-butanone, 3.6 g (48 mmol) of 2-(methylamino)ethanol and 6.6 g (48 mmol) of potassium carbonate is heated to 70° C. for 5 h.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US04914092 |
| Source dataset | uspto-grants-1990_04 |
| ORD ID | ord-3c3f4f5e6e19474282e52d69a70037bf |
| Source note | uspto-grants-1990_04 |