HuagongsheHuagongshe Chemistry Print Report · For research reference only
Benzoyl Peroxide → HCID 13648813, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Benzoyl Peroxide | HCID 7187 | — |
| Reactant | Chlorosuccinimide | HCID 31398 | — |
| Reactant | HCID 13457646 | HCID 13457646 | — |
| Solvent | Carbon Tetrachloride | HCID 5943 | — |
| Product | HCID 13648813 | HCID 13648813 | — |
Reaction Steps
A mixture of 2,4-dichloro-6-phenylimidazo[1,5-a]pyrimidine (0.88 g), N-chlorosuccinimide (0.5 g) and benzoyl peroxide (0.04 g) in carbon tetrachloride (20 ml) was heated to reflux for 14 hours. The mixture was concentrated and purified by alumina column chromatography, eluting with benzene to give the objective product which was recrystallized from ethanol to yellow plates (0.32 g), mp 133°-134° C.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US04914104 |
| Source dataset | uspto-grants-1990_04 |
| ORD ID | ord-491132ad6dff42ce94a2aa62a1f9e007 |
| Source note | uspto-grants-1990_04 |