HuagongsheHuagongshe Chemistry Print Report · For research reference only
(Dimethyl sulfide)trihydroboron → HCID 12945116, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | (Dimethyl sulfide)trihydroboron | HCID 12423031 | — |
| Reactant | HCID 19913608 | HCID 19913608 | — |
| Product | HCID 12945116 | HCID 12945116 | — |
Reaction Steps
4-[1,1-Dimethylethyl]-2-phenylmorpholine was prepared from 4-[1,1-dimethylethyl]-5-oxo-2-phenylmorpholine and borane-methyl sulphide by an analogous procedure to that described in Example 1. After purification by column chromatography on silica using 0->8% methanol in dichloromethane as eluant, the resultant oil was converted to its hydrochloride salt, m.p. 208°-210° C., (ethyl acetate).
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US04914202 |
| Source dataset | uspto-grants-1990_04 |
| ORD ID | ord-a5632580c4b94e75a04df07db6777fcb |
| Source note | uspto-grants-1990_04 |