Thionyl Chloride → HCID 19860557, compound

Participants

Reaction Steps

Quinoline-8-carboxylic acid (1.0 g) was added to 3 ml of thionyl chloride, and the reaction mixture heated at reflux for one hour. The reaction mixture was allowed to stir at room temperature and was then concentrated in vacuo. The residue was washed with benzene (2×10 ml) and was used in the next reaction.

Provenance & Evidence