HuagongsheHuagongshe Chemistry Print Report · For research reference only
1H-Benzimidazole-2-acetonitrile → 2-(1H-1,3-benzodiazol-2-yl)ethanethioamide
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | 1H-Benzimidazole-2-acetonitrile | HCID 20455 | — |
| Reactant | Diethyldithiophosphate | HCID 53249491 | — |
| Solvent | Dimethylformamide | HCID 6228 | — |
| Product | 2-(1H-1,3-benzodiazol-2-yl)ethanethioamide | HCID 4962538 | — |
Reaction Steps
Using the procedure of Preparation A3, 2.0 g of 2-benzimidazoleacetonitrile and 2.3 ml of diethyl dithiophosphate in 10 ml of dimethylformamide gave 150 mg of the titled compound.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US04914207 |
| Source dataset | uspto-grants-1990_04 |
| ORD ID | ord-fcc0251ac4f1471abddb626446621957 |
| Source note | uspto-grants-1990_04 |