Propylene Glycol → HCID 19860675, compound

HRID 2072858Notes

Reaction equation

HRID 2072858 reaction equation
[OH:1][CH2:2][CH:3]([OH:5])[CH3:4].[N+:6]([C:9]1[CH:14]=[CH:13][CH:12]=[CH:11][C:10]=1Cl)([O-:8])=[O:7].[OH-:16].[Na+]>CS(C)=O>[N+:6]([C:9]1[CH:14]=[CH:13][C:12]([O:1][CH2:2][CH:3]([O:5][C:12]2[CH:13]=[CH:14][C:9]([N+:6]([O-:7])=[O:16])=[CH:10][CH:11]=2)[CH3:4])=[CH:11][CH:10]=1)([O-:8])=[O:7]

Participants

5

Reactant 3

HCID 1030Propylene GlycolHCID 69451-Chloro-2-nitrobenzeneHCID 14798Sodium Hydroxide

Product 1

HCID 19860675HCID 19860675, compound

Reagents, catalysts & solvents 1

HCID 679Dimethyl SulfoxideSolvent

Procedure

76 g (1 mol) 1,2-dihydroxypropane, 346.5 g (2.2 mols) nitrochlorobenzene and 140 g powdered sodium hydroxide were reacted following the procedure described in Example 1 in 600 ml DMSO.

Workup

  1. customwere reacted

Sources & evidence

ORD record
ord-02941a41e96540548dfcedf3b7707467
Source dataset
uspto-grants-1990_04
Patent number
US04914238

Reaction notes

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