1-Chloro-2-nitrobenzene → HCID 19860684, compound

HRID 2072861Notes

Reaction equation

HRID 2072861 reaction equation
[OH:1][CH2:2][C:3]([CH3:7])([CH2:5][OH:6])[CH3:4].[N+:8]([C:11]1[CH:16]=[CH:15][CH:14]=[CH:13][C:12]=1Cl)([O-:10])=[O:9].[OH-:18].[Na+]>CS(C)=O>[N+:8]([C:11]1[CH:16]=[CH:15][CH:14]=[CH:13][C:12]=1[O:1][CH2:2][C:3]([CH3:7])([CH3:4])[CH2:5][O:6][C:12]1[CH:13]=[CH:14][CH:15]=[CH:16][C:11]=1[N+:8]([O-:9])=[O:18])([O-:10])=[O:9]

Participants

5

Reactant 3

HCID 69451-Chloro-2-nitrobenzeneHCID 14798Sodium HydroxideHCID 31344Neopentyl glycol

Product 1

HCID 19860684HCID 19860684, compound

Reagents, catalysts & solvents 1

HCID 679Dimethyl SulfoxideSolvent

Procedure

104 g (1 mol) neopentyl glycol, 346.5 g (2.2 mols) 2-nitrochlorobenzene and 140 g powdered sodium hydroxide were reacted following the procedure described in Example 1 in 600 ml DMSO.

Workup

  1. customwere reacted

Sources & evidence

ORD record
ord-1de418dfb56941368100d415d9af6df3
Source dataset
uspto-grants-1990_04
Patent number
US04914238

Reaction notes

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