HuagongsheHuagongshe Chemistry Print Report · For research reference only
HCID 19860684, compound → HCID 19860670, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | HCID 19860684 | HCID 19860684 | — |
| Reactant | HCID 178418361 | HCID 178418361 | — |
| Catalyst | Nickel | HCID 935 | — |
| Solvent | Dimethylformamide | HCID 6228 | — |
| Product | HCID 19860670 | HCID 19860670 | — |
Reaction Steps
343 g 1,3-bis(2-nitrophenoxy)-2,2-dimethylpropane were hydrogenated at 60° C./50 bar in 1800 ml DMF in the presence of 53 g Raney nickel. After the uptake of hydrogen had stopped, the catalyst was filtered off and the solvent was removed in vacuo.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US04914238 |
| Source dataset | uspto-grants-1990_04 |
| ORD ID | ord-1b135adb3cd5478897cc294858f8ea8e |
| Source note | uspto-grants-1990_04 |