HuagongsheHuagongshe Chemistry Print Report · For research reference only
Hydrochloric Acid → HCID 23037335, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Hydrochloric Acid | HCID 313 | — |
| Reactant | HCID 14390292 | HCID 14390292 | — |
| Solvent | Isopropanol | HCID 3776 | — |
| Product | HCID 23037335 | HCID 23037335 | — |
Reaction Steps
2-(4-Bromophenyl)-N-[2-(dimethylamino)ethyl]-3H-imidazo[4,5-b]pyridine-3-acetamide (2.25 g, 0.0056 mole) was treated with concentrated hydrochloric acid and isopropyl alcohol to give 2.4 g precipitate. Recrystallization from isopropyl alcohol gave 1.9 g (70%) of white solid, mp 160.5°-162° C.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US04914109 |
| Source dataset | uspto-grants-1990_04 |
| ORD ID | ord-d262b8bfa44a48f3b085195910977a2e |
| Source note | uspto-grants-1990_04 |