HuagongsheHuagongshe Chemistry Print Report · For research reference only
Methanol → HCID 23365355, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Methanol | HCID 887 | — |
| Reactant | Potassium Hydroxide | HCID 14797 | — |
| Reactant | HCID 23365288 | HCID 23365288 | — |
| Product | HCID 23365355 | HCID 23365355 | — |
Reaction Steps
1.5 g of 4-(4-bromobenzyloxy)-3-[1-(1-imidazolyl)butyl]-benzonitrile (of example 3) is reacted with 3 g of potassium hydroxide in an aqueous methanol solution for 24 hours under reflux. After working up, 1.1 g of 4-(4-bromobenzyloxy)-3-[1-(1-imidazolyl)-butyl]-benzoic acid with a melting point of 187°-189° C. is obtained.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US04916144 |
| Source dataset | uspto-grants-1990_04 |
| ORD ID | ord-0183e6af9d494b769526e7244658b8d9 |
| Source note | uspto-grants-1990_04 |