Benzoyl chloride → HCID 70356478, compound

HRID 2073243Notes

Reaction equation

HRID 2073243 reaction equation
[NH2:1][C:2]1[CH:7]=[C:6]([C:8]([F:11])([F:10])[F:9])[CH:5]=[CH:4][C:3]=1[N:12]([C:14](=[O:16])[CH3:15])[NH2:13].[C:17](Cl)(=[O:24])[C:18]1[CH:23]=[CH:22][CH:21]=[CH:20][CH:19]=1>N1C=CC=CC=1>[C:17]([NH:1][C:2]1[CH:7]=[C:6]([C:8]([F:11])([F:10])[F:9])[CH:5]=[CH:4][C:3]=1[N:12]([C:14](=[O:16])[CH3:15])[NH2:13])(=[O:24])[C:18]1[CH:23]=[CH:22][CH:21]=[CH:20][CH:19]=1

Participants

4

Reactant 2

HCID 7412Benzoyl chlorideHCID 70356581HCID 70356581, compound

Product 1

HCID 70356478HCID 70356478, compoundYield 93.6%

Reagents, catalysts & solvents 1

HCID 1049PyridineSolvent

Procedure

The process of Example 14 was followed by using 66.5 g of 2-amino-4-trifluoromethyl-N-acetylphenylhydrazine, 70 ml of pyridine and 32.9 ml of benzoyl chloride as starting materials to yield 90 g (93.6%) of 2-benzoylamino-4-trifluoromethyl-N-acetylphenylhydrazine, m.p.: 212°-214° C. after recrystallization from 96% ethanol.

Sources & evidence

ORD record
ord-f4f515acae1c460aa26e124d6caa13f5
Source dataset
uspto-grants-1990_04
Patent number
US04916149

Reaction notes

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