HuagongsheHuagongshe Chemistry Print Report · For research reference only
Benzoyl chloride → HCID 70356478, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Benzoyl chloride | HCID 7412 | — |
| Reactant | HCID 70356581 | HCID 70356581 | — |
| Solvent | Pyridine | HCID 1049 | — |
| Product | HCID 70356478 | HCID 70356478 | 93.6% |
Reaction Steps
The process of Example 14 was followed by using 66.5 g of 2-amino-4-trifluoromethyl-N-acetylphenylhydrazine, 70 ml of pyridine and 32.9 ml of benzoyl chloride as starting materials to yield 90 g (93.6%) of 2-benzoylamino-4-trifluoromethyl-N-acetylphenylhydrazine, m.p.: 212°-214° C. after recrystallization from 96% ethanol.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US04916149 |
| Source dataset | uspto-grants-1990_04 |
| ORD ID | ord-f4f515acae1c460aa26e124d6caa13f5 |
| Source note | uspto-grants-1990_04 |