HuagongsheHuagongshe Chemistry Print Report · For research reference only
HCID 14570084, compound → HCID 14570085, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | HCID 14570084 | HCID 14570084 | — |
| Catalyst | Palladium | HCID 23938 | — |
| Solvent | Ethanol | HCID 702 | — |
| Product | HCID 14570085 | HCID 14570085 | 58.2% |
Reaction Steps
A solution of 7.8 g of 3'-(phenylmethoxy)-N-[4-(3-pyridinyl)butyl][1,1'-biphenyl]-4-carboxamide in 150 mL of ethanol was hydrogenated over 0.8 g of 10% palladium on carbon. The product was crystallized from acetonitrile to give 3.6 g of 3'-hydroxy-N-[4-(3-pyridinyl)butyl][1,1'-biphenyl]-4-carboxamide mp 150°-151.5° C. The analytical sample was obtained from acetonitrile, mp 151.5°-152.5° C.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US04916145 |
| Source dataset | uspto-grants-1990_04 |
| ORD ID | ord-16c671e31b2e41be9908a3beae5d421a |
| Source note | uspto-grants-1990_04 |