HCID 72744946, compound → HCID 54375492, compound

Participants

Reaction Steps

As in Example 133, hydrolysis of 3.88 g of (R,S)-Z]-[1-methyl-4-(3-Pyridinyl)-3-butenyl]carbamic acid 1,1-dimethylethyl ester in 50 mL of 1N HCl yielded, after the usual work-up and evaporative distillation of the product (100-120° C./0.1 mm), 1.7 g of [(R,S)-Z]-1-methyl-4-(3-pyridinyl)-3-butenamine as an oil.

Provenance & Evidence