HuagongsheHuagongshe Chemistry Print Report · For research reference only
Potassium Carbonate → HCID 19858315, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Potassium Carbonate | HCID 11430 | — |
| Reactant | Iodoethanol | HCID 12225 | — |
| Reactant | 1-Propene, 1-methoxy- | HCID 111290 | — |
| Catalyst | Phosphorus oxychloride | HCID 24813 | — |
| Product | HCID 19858315 | HCID 19858315 | — |
Reaction Steps
To 6 mls of cold (0° C.) methoxypropene was added 3 mls of 2-iodoethanol and 1 drop of phosphorous oxychloride (POCl3). The reaction was stirred for 1 hour and then solid potassium carbonate was added. After 10 minutes the liquid was decanted and was concentrated to obtain the product as an oil.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US04916223 |
| Source dataset | uspto-grants-1990_04 |
| ORD ID | ord-dcbd2b7f849f4c2696fe0f4e061058ad |
| Source note | uspto-grants-1990_04 |