HuagongsheHuagongshe Chemistry Print Report · For research reference only
Bromine → HCID 19858071, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Bromine | HCID 24408 | — |
| Reactant | HCID 54424481 | HCID 54424481 | — |
| Solvent | Acetic Acid | HCID 176 | — |
| Product | HCID 19858071 | HCID 19858071 | — |
Reaction Steps
A solution of bromine (0.05 ml) in acetic acid (2 ml) was added over 5 minutes to a solution of 2-hydroxy-7-methyl-1-naphthylacetic acid (0.21 g) in acetic acid (5 ml). The solid which precipitated was collected and washed with acetic acid to give 7-bromo-8-methyl-2(1H)-naphtho[2,1-b]furanone, m.p. 238°-240°.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US04916148 |
| Source dataset | uspto-grants-1990_04 |
| ORD ID | ord-a94175d01793431a86413bf52d98c224 |
| Source note | uspto-grants-1990_04 |