HRID2073459

反应详情

EQUATION

反应方程式

HRID 2073459 的结构方程式

CONDITIONS

反应条件

温度
140 °C

PROCEDURE

实验过程

In a similar manner to that described in Example 1, o-allylphenol (134 g), 1,3-bisglycidylresorcinol (115.1 g), triphenylethylphosphonium iodide (0.75 g) and methylglycolate (145 g) were reacted at 100° C. for 13 hours. The solvent and excess o-allylphenol were removed by heating at 140° C. finally in vacuo. The yield of adduct was 227.9 g and it showed a viscocity of 280 mPa.s at 70° C.

WORKUP

后处理

  1. customwere reacted at 100° C. for 13 hours
  2. customThe solvent and excess o-allylphenol were removed
  3. customat 70° C.