Thionyl Chloride → HCID 22996574, compound

HRID 2073483Notes

Reaction equation

HRID 2073483 reaction equation
[F:1][C:2]1[CH:7]=[CH:6][C:5]([CH:8]([C:12]2[CH:17]=[CH:16][C:15]([F:18])=[CH:14][CH:13]=2)[C:9](O)=[O:10])=[CH:4][CH:3]=1.S(Cl)([Cl:21])=O>>[F:1][C:2]1[CH:7]=[CH:6][C:5]([CH:8]([C:12]2[CH:17]=[CH:16][C:15]([F:18])=[CH:14][CH:13]=2)[C:9]([Cl:21])=[O:10])=[CH:4][CH:3]=1

Participants

3

Reactant 2

HCID 24386Thionyl ChlorideHCID 135116842,2-Bis(4-fluorophenyl)acetic acid

Product 1

HCID 22996574HCID 22996574, compound

Procedure

35.5 g (0.143 mol) of bis(4-fluorophenyl)acetic acid were stirred at the reflux temperature in 150 ml of thionyl chloride for 4.5 hours and the excess thionyl chloride was evaporated off in vacuo.

Workup

  1. customthe excess thionyl chloride was evaporated off in vacuo

Sources & evidence

ORD record
ord-b5a02230d0764cd586c5768deb12a963
Source dataset
uspto-grants-1990_04
Patent number
US04918073

Reaction notes

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