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HuagongsheHuagongshe Chemistry Print Report · For research reference only
HRID 2073483Generated: October 30, 2026

Thionyl Chloride → HCID 22996574, compound

https://huagongshe.com/reaction/2073483

Reaction equation

Participants

RoleNameHCIDCharge
ReactantThionyl ChlorideHCID 24386—
Reactant2,2-Bis(4-fluorophenyl)acetic acidHCID 13511684—
ProductHCID 22996574HCID 22996574—

Reaction Steps

35.5 g (0.143 mol) of bis(4-fluorophenyl)acetic acid were stirred at the reflux temperature in 150 ml of thionyl chloride for 4.5 hours and the excess thionyl chloride was evaporated off in vacuo.

Provenance & Evidence

DOI10.6084/m9.figshare.5104873.v1
Patent numberUS04918073
Source datasetuspto-grants-1990_04
ORD IDord-b5a02230d0764cd586c5768deb12a963
Source noteuspto-grants-1990_04