HuagongsheHuagongshe Chemistry Print Report · For research reference only
Potassium Iodide → HCID 19857169, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Potassium Iodide | HCID 4875 | — |
| Reactant | 1-Piperazinecarboxylic acid, ethyl ester | HCID 8431 | — |
| Reactant | Potassium Carbonate | HCID 11430 | — |
| Reactant | HCID 19857181 | HCID 19857181 | — |
| Solvent | Methyl Isobutyl Ketone | HCID 7909 | — |
| Product | HCID 19857169 | HCID 19857169 | — |
Reaction Steps
50 g (0.17 mol) of 4,5-bis(4-fluorophenyl)pentyl chloride, 32.5 g (0.21 mol) of ethyl piperazine-1-carboxylate, 46.9 g (0.34 mol) of powdered potassium carbonate and 2.8 g of potassium iodide were reacted in 580 ml of methyl isobutyl ketone and the mixture was worked up, by a process analogous to that described in Example 3d).
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US04918073 |
| Source dataset | uspto-grants-1990_04 |
| ORD ID | ord-cc8624ffbf294356a488ae190a2f277e |
| Source note | uspto-grants-1990_04 |