HuagongsheHuagongshe Chemistry Print Report · For research reference only
HCID 19857187, compound → HCID 19857167, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | HCID 19857187 | HCID 19857187 | — |
| Catalyst | Palladium | HCID 23938 | — |
| Solvent | Methanol | HCID 887 | — |
| Product | HCID 19857167 | HCID 19857167 | — |
Reaction Steps
17 g (40.7 mmol) of 1-benzyl-4-[4,4-bis(4-fluorophenyl)-butylidene]piperidine were hydrogenated in 850 ml of methanol with 5 g of palladium-on-charcoal (10%) at 45° C. in a shaking vessel for 2 hours. The catalyst was filtered off with suction and the solution was concentrated.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US04918073 |
| Source dataset | uspto-grants-1990_04 |
| ORD ID | ord-a7996edd6a2b4c1e969349a076513a33 |
| Source note | uspto-grants-1990_04 |