HuagongsheHuagongshe Chemistry Print Report · For research reference only
HCID 54466938, compound → HCID 135698649, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | HCID 54466938 | HCID 54466938 | — |
| Reactant | HCID 178418311 | HCID 178418311 | — |
| Solvent | Ethanol | HCID 702 | — |
| Product | HCID 135698649 | HCID 135698649 | 44.9% |
Reaction Steps
A mixture of 50 g of methyl 2-acetyl-3-(2-thienyl)acrylate, 20 g of 3-amino-1,2,4-triazole and 300 ml of ethanol is heated under reflux for 4 hours. The precipitated white crystals are collected by filtration to give 29.5 g of 6-methoxycarbonyl-5-methyl-7-(2-thienyl)-4,7-dihydro-1,2,4-triazolo[1,5-a]pyrimidine, melting at 239°-240° C.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US04918074 |
| Source dataset | uspto-grants-1990_04 |
| ORD ID | ord-a05103b283214cb7bc22dfd207842079 |
| Source note | uspto-grants-1990_04 |