HuagongsheHuagongshe Chemistry Print Report · For research reference only
Methyl (4,6-dimethoxypyrimidin-2-yl)carbamate → HCID 15077136, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Methyl (4,6-dimethoxypyrimidin-2-yl)carbamate | HCID 13314628 | — |
| Reactant | 5-Ethoxy-2-methyl-1,3-thiazole-4-sulfonamide | HCID 15077123 | — |
| Reactant | Trimethylaluminum | HCID 16682925 | — |
| Product | HCID 15077136 | HCID 15077136 | 49.7% |
Reaction Steps
By employing the procedure described in Example 2, the reaction of 1.33 g of 5-ethoxy-2-methyl-4-thiazolesulfonamide with 1.4 g of methyl N-(4,6-dimethoxypyrimidin-2-yl)carbamate in the presence of 3.3 ml of a 2.0M solution of trimethylaluminum, there was obtained 1.2 g of the title compound, m.p. 140°-143°. IR: 1710 cm-1 (C=O).
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US04919706 |
| Source dataset | uspto-grants-1990_04 |
| ORD ID | ord-f25b56920c35439c95556f8cbc1e290e |
| Source note | uspto-grants-1990_04 |