3,4-Dimethoxybenzeneacetonitrile → Homoveratrylamine

HRID 2073735Notes

Reaction equation

HRID 2073735 reaction equation
[CH3:1][O:2][C:3]1[CH:4]=[C:5]([CH2:11][C:12]#[N:13])[CH:6]=[CH:7][C:8]=1[O:9][CH3:10].[H-].[Al+3].[Li+].[H-].[H-].[H-]>>[CH3:1][O:2][C:3]1[CH:4]=[C:5]([CH2:11][CH2:12][NH2:13])[CH:6]=[CH:7][C:8]=1[O:9][CH3:10]

Participants

3

Reactant 2

HCID 667273,4-DimethoxybenzeneacetonitrileHCID 21226445Aluminium lithium hydride

Product 1

HCID 8421Homoveratrylamine

Procedure

In a manner similar to Preparation 2 react 3,4-dimethoxybenzeneacetonitrile with lithium aluminum hydride to obtain the title compound.

Workup

  1. customIn a manner similar to Preparation 2

Sources & evidence

ORD record
ord-b81f62c8b6284a6c9944c739b71177bf
Source dataset
uspto-grants-1990_04
Patent number
US04920116

Reaction notes

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