HuagongsheHuagongshe Chemistry Print Report · For research reference only
HCID 19855899, compound → HCID 19855943, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | HCID 19855899 | HCID 19855899 | — |
| Catalyst | Palladium | HCID 23938 | — |
| Solvent | Ethanol | HCID 702 | — |
| Product | HCID 19855943 | HCID 19855943 | — |
Reaction Steps
Hydrogenate N-(4-fluorophenyl)-4-[(methylsulfonyl)amino]-N-[2-[(2-phenylethyl)(phenylmethyl)amino]ethyl]benzamide hydrochloride over palladium on carbon in ethanol at 30-40 psi. Follow the progress of the reaction by thinlayer chromatography on silica gel. At the completion of the reaction remove the catalyst by filtration and evaporate the solvent in vacuo to obtain the title compound.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US04920116 |
| Source dataset | uspto-grants-1990_04 |
| ORD ID | ord-3bfc42208e98411c9c1ff6dfbd513b9e |
| Source note | uspto-grants-1990_04 |