HRID2073796

反应详情

EQUATION

反应方程式

HRID 2073796 的结构方程式

AUXILIARIES

试剂、催化剂与溶剂

1

PROCEDURE

实验过程

A solution of potassium cyanate (1.62 g) in water (5 ml) was added dropwise to a mixture of 2-amino-6-methylbenzyl alcohol (1.37 g), water (5 ml), and acetic acid (6 ml) at room temperature. After being stirred for 2.5 hours, the resulting precipitates were collected by filtration, washed with water, and dried to give 2-methyl-6-ureidobenzyl alcohol (1.33 g).

WORKUP

后处理

  1. customthe resulting precipitates
  2. filtrationwere collected by filtration
  3. washwashed with water
  4. customdried