HuagongsheHuagongshe Chemistry Print Report · For research reference only
Acetic Acid → 2-Methyl-6-ureidobenzyl alcohol
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Acetic Acid | HCID 176 | — |
| Reactant | Potassium cyanate | HCID 11378442 | — |
| Reactant | (2-Amino-6-methylphenyl)methanol | HCID 15339417 | — |
| Solvent | Water | HCID 962 | — |
| Product | 2-Methyl-6-ureidobenzyl alcohol | HCID 14368456 | 73.9% |
Reaction Steps
A solution of potassium cyanate (1.62 g) in water (5 ml) was added dropwise to a mixture of 2-amino-6-methylbenzyl alcohol (1.37 g), water (5 ml), and acetic acid (6 ml) at room temperature. After being stirred for 2.5 hours, the resulting precipitates were collected by filtration, washed with water, and dried to give 2-methyl-6-ureidobenzyl alcohol (1.33 g).
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US04920129 |
| Source dataset | uspto-grants-1990_04 |
| ORD ID | ord-d46755e0e6a64c30bf1e71ec7bde811e |
| Source note | uspto-grants-1990_04 |