HuagongsheHuagongshe Chemistry Print Report · For research reference only
Thionyl Chloride → HCID 14368348, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Thionyl Chloride | HCID 24386 | — |
| Reactant | 2-Methyl-6-ureidobenzyl alcohol | HCID 14368456 | — |
| Solvent | Dichloromethane | HCID 6344 | — |
| Product | HCID 14368348 | HCID 14368348 | 59.9% |
Reaction Steps
A mixture of 2-methyl-6-ureidobenzyl alcohol (1 g) and thionyl chloride (0.66 g) in methylene chloride (20 ml) was stirred for 2 hours at room temperature and evaporated in vacuo. The residue was washed with water and dried in a desiccator to give 2-methyl-6-ureidobenzyl chloride (0.66 g).
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US04920129 |
| Source dataset | uspto-grants-1990_04 |
| ORD ID | ord-48fe8fb720834df79d6fe6d6721b51c3 |
| Source note | uspto-grants-1990_04 |