HuagongsheHuagongshe Chemistry Print Report · For research reference only
Ammonium Hydroxide → HCID 14800670, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Ammonium Hydroxide | HCID 14923 | — |
| Reactant | HCID 14800669 | HCID 14800669 | — |
| Solvent | Tetrahydrofuran | HCID 8028 | — |
| Product | HCID 14800670 | HCID 14800670 | — |
Reaction Steps
3-(4-(2-Quinolinylmethyloxy)benzyl)benzoyl chloride (0.05 mol) in tetrahydrofuran (300 ml) is treated with concentrated ammonium hydroxide (25 ml). The reaction mixture is stirred overnight at room temperature and then evaporated and partitioned between ethyl acetate and water. The ethyl acetate fraction is dried and evaporated to give 3-(4-(2-quinolinylmethyloxy)benzyl)benzamide.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US04920133 |
| Source dataset | uspto-grants-1990_04 |
| ORD ID | ord-720298537d57402a9ac60946355ead25 |
| Source note | uspto-grants-1990_04 |