Hydrochloric Acid → HCID 86743876, compound

HRID 2073914Notes

Reaction equation

HRID 2073914 reaction equation
[CH:1]([C:5]1[CH:10]=[CH:9][C:8]([OH:11])=[CH:7][CH:6]=1)([CH2:3][CH3:4])[CH3:2].[C:12]1([CH3:21])[CH:17]=[CH:16][CH:15]=[C:14]([CH:18]=[O:19])[C:13]=1[CH3:20].Cl>>[CH:1]([C:5]1[CH:6]=[CH:7][C:8]([OH:11])=[CH:9][CH:10]=1)([CH2:3][CH3:4])[CH3:2].[C:12]1([CH3:21])[CH:17]=[CH:16][CH:15]=[C:14]([CH:18]=[O:19])[C:13]=1[CH3:20]

Participants

4

Reactant 3

HCID 313Hydrochloric AcidHCID 74534-sec-ButylphenolHCID 342242,3-Dimethylbenzaldehyde

Product 1

HCID 86743876HCID 86743876, compound

Conditions

Temperature
100 °C

Procedure

A mixture composed of 30 parts of p-sec-butylphenol, 100 parts of xylene-formaldehyde resin (Nikanol-H made by Mitsubishi Gas Chemical Co., Ltd.), and 1 part of conc. hydrochloric acid (35%) was heated at 100° C. for 6 hours. The reaction produce was washed with hot water to remove hydrochloric acid and freed of water by distillation under reduced pressure. Thus, there was obtained 124 parts of p-sec-butylphenol-xylene-formaldehyde resin.

Workup

  1. customThe reaction produce
  2. washwas washed with hot water
  3. customto remove hydrochloric acid
  4. distillationfreed of water by distillation under reduced pressure

Sources & evidence

ORD record
ord-d7fadc8ad43f479ebb462b75608e6a91
Source dataset
uspto-grants-1990_04
Patent number
US04920185

Reaction notes

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