Participants
| Role | Name | HCID | Charge |
|---|
| Reactant | Methylamine | HCID 6329 | — |
| Reactant | Methyl 3-{[(1-ethoxyethylidene)amino]oxy}propanoate | HCID 71331645 | — |
| Solvent | Methanol | HCID 887 | — |
| Product | HCID 57869858 | HCID 57869858 | 100% |
Reaction Steps
To a solution of a known compound, 3-(1-ethoxyethylideneaminooxy)-propanoic acid methyl ester (CAS No. 97164-30-2, 41.3 g, 0.218 mol) in methanol (150 ml) was added methylamine (40% solution in methanol, 200 ml) at room temperature, and the mixture was stirred at 60° C. for 12 hours. The reaction mixture was concentrated under reduced pressure to give N-(2-methylcarbamoyl-ethoxy)-acetimidic acid ethyl ester (41.0 g, 100%).
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|
| Patent number | US07745663B2 |
|---|
| Source dataset | uspto-grants-2010_06 |
|---|
| ORD ID | ord-0f42f8336615425993af73d3ecc9da46 |
|---|
| Source note | uspto-grants-2010_06 |
|---|
