HuagongsheHuagongshe Chemistry Print Report · For research reference only
Ethanol → HCID 86600963, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Ethanol | HCID 702 | — |
| Reactant | HCID 67089774 | HCID 67089774 | — |
| Catalyst | Palladium | HCID 23938 | — |
| Product | HCID 86600963 | HCID 86600963 | — |
Reaction Steps
To a solution of N′-{(R)-2-[(Benzyloxyformylamino)methyl]heptanoyl]-hydrazinecarboxylic acid benzyl ester (1 mmol) in EtOH (10 mL) was added 10% Pd/C (50 mg). The mixture was subjected to hydrogenation for 5 hours at room temperature and then filtered through Celite. The filtrate was evaporated and purified by hplc to afford N-[(R)-2-(Hydrazinocarbonyl)-heptyl]-N-hydroxy-formamide as a glass. MH+218.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US07919528B2 |
| Source dataset | uspto-grants-2011_04 |
| ORD ID | ord-dbb3c125381d4ce7bf477bb2d16713f5 |
| Source note | uspto-grants-2011_04 |