Acetic Acid → HCID 58926503, compound

Participants

Reaction Conditions

Reaction Steps

7-Bromo-1-phenyl-[1,2,4]triazolo[4,3-a]quinoxaline (7.4 g, 22.7 mmol), hydrogen peroxide (30%, 59 mL), and acetic acid (185 mL) were combined and heated at 50° C. overnight. Additional hydrogen peroxide (30%, 15 mL) was added to push the reaction to completion, and the mixture was stirred overnight at room temperature. The reaction was added to water (550 mL) and the precipitate was filtered and rinsed with water to give the desired product, 7a.

Provenance & Evidence