Hydroxyamine hydrochloride → HCID 58257762, compound

Participants

Reaction Steps

10p (990 mg, 15.5 mmol), hydroxylamine hydrochloride (220 mg, 31.1 mmol), and potassium acetate (310 mg, 31.1 mmol) were dissolved in MeOH (1.5 mL) and stirred overnight at room temperature. The reaction was concentrated and purified by silica gel chromatography (30% EtOAc in hexanes) to give the desired product, 10q.

Provenance & Evidence