HuagongsheHuagongshe Chemistry Print Report · For research reference only
Methanol → HCID 823415, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Methanol | HCID 887 | — |
| Reactant | HCID 25179628 | HCID 25179628 | — |
| Product | HCID 823415 | HCID 823415 | 94.7% |
Reaction Steps
A mixture of 137 g of N-phenyl-4-chlorocarbonylphthalimide and methanol (1.37 L) was refluxed for 1 hr. The solid which formed on cooling was collected and dried to afford 128 g (94.7%) of N-phenyl-4-carbomethoxyphthalimide, Compound 1, mp 200-207° C. Recrystallization of 91.3 g from 2 L of acetonitrile yielded 77.8 g (80.7%) of Compound 1, mp 205-207° C.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US07923184B2 |
| Source dataset | uspto-grants-2011_04 |
| ORD ID | ord-9d2f3cb9f3744e619ef72b939657c93e |
| Source note | uspto-grants-2011_04 |