HuagongsheHuagongshe Chemistry Print Report · For research reference only
HCID 67095819, compound → HCID 57780696, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | HCID 67095819 | HCID 67095819 | — |
| Reactant | HCID 178493228 | HCID 178493228 | — |
| Product | HCID 57780696 | HCID 57780696 | — |
Reaction Steps
The title compound was prepared from 6-[1-dimethylamino-methylidene]-2-(3,4-dichloro-phenyl)-cyclohexanone (119 mg, 0.40 mmol) and N-[3-methoxy-4-(4-methyl-imidazol-1-yl)-phenyl]-guanidine dinitrate (148 mg, 0.40 mmol) using in analogous manner the procedure described in example 45b). Obtained as an off-white solid (92 mg, 48%). MS ISP (m/e): 480.0 [(M+H)+]. mp 167-169° C.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US07923450B2 |
| Source dataset | uspto-grants-2011_04 |
| ORD ID | ord-d84395df884048c095a9dbd3a57510f0 |
| Source note | uspto-grants-2011_04 |