HuagongsheHuagongshe Chemistry Print Report · For research reference only
HCID 67095891, compound → HCID 57780708, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | HCID 67095891 | HCID 67095891 | — |
| Reactant | HCID 178493228 | HCID 178493228 | — |
| Product | HCID 57780708 | HCID 57780708 | — |
Reaction Steps
The title compound was prepared from crude methyl 5-[1-dimethylamino-methylidene]-4-oxo-tetrahydro-pyran-3-carboxylate (97 mg, 0.45 mmol) and N-[3-methoxy-4-(4-methyl-imidazol-1-yl)-phenyl]-guanidine dinitrate (114 mg, 0.31 mmol) using in analogous manner the procedure described in example 45b). Obtained as a pale-yellow oil (8 mg, 7%). MS ISP (m/e): 396.4 [(M+H)+].
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US07923450B2 |
| Source dataset | uspto-grants-2011_04 |
| ORD ID | ord-4c47b7105b1c4b61ac8927d9345d8845 |
| Source note | uspto-grants-2011_04 |