HuagongsheHuagongshe Chemistry Print Report · For research reference only
HCID 67096271, compound → HCID 57780687, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | HCID 67096271 | HCID 67096271 | — |
| Reactant | HCID 178493228 | HCID 178493228 | — |
| Product | HCID 57780687 | HCID 57780687 | — |
Reaction Steps
The title compound was prepared from crude ethyl 2-(2,5-dichloro-phenyl)-7-[1-dimethylamino-methylidene]-cycloheptanone (197 mg, ca. 0.61 mmol) and N-[3-methoxy-4-(4-methyl-imidazol-1-yl)-phenyl]-guanidine dinitrate (169 mg, 0.45 mmol) using in analogous manner the procedure described in example 45b). Obtained as a pale-yellow solid (163 mg, 73%). MS ISP (m/e): 494.0 [(M+H)+]. mp 218-220° C.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US07923450B2 |
| Source dataset | uspto-grants-2011_04 |
| ORD ID | ord-0af74c6671164c7d87455d209e83b95a |
| Source note | uspto-grants-2011_04 |