HuagongsheHuagongshe Chemistry Print Report · For research reference only
HCID 67096148, compound → HCID 57780705, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | HCID 67096148 | HCID 67096148 | — |
| Reactant | [3-methoxy-4-(4-methyl-1H-imidazol-1-yl)phenyl]thiourea | HCID 71650841 | — |
| Product | HCID 57780705 | HCID 57780705 | — |
Reaction Steps
The title compound was prepared from [3-methoxy-4-(4-methyl-imidazol-1-yl)-phenyl]-thiourea (70 mg, 0.27 mmol) and crude 2-bromo-6-(3-methyl-[1,2,4]oxadiazol-5-yl)-cyclohexanone (173 mg, ca. 0.5 mmol) using in analogous manner the procedure described in example 1b). Obtained as a light-brown foam (25 mg, 22%). MS ISP (m/e): 423.1 (100) [(M+H)+].
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US07923450B2 |
| Source dataset | uspto-grants-2011_04 |
| ORD ID | ord-464e7d2d55ac4f7da4ad5392fcdf20bc |
| Source note | uspto-grants-2011_04 |