1-Methylpyrrolidine → HCID 19704841, compound

Participants

Reaction Steps

Twenty-five grams of trifluoromethanesulfonic acid was added dropwise to a solution of 14.2 g of 1-methylpyrrolidine in 25 ml of ethanol at 0° C. The solution was returned to room temperature, stirred overnight, and dried in vacuo at 60° C. for 16 hours to furnish 1-methylpyrrolidine trifluoromethanesulfonate (MePy+TfS−) as a brown solid. The resulting salt had a melting point of 97.5° C.

Provenance & Evidence