Huagongshe화공사 화학 정보 인쇄 보고서 · 연구 참고용
Suberic acid → Oxonane-2,9-dione
참여 물질
| 역할 | 이름 | HCID | 투입량 |
|---|---|---|---|
| 반응물 | Suberic acid | HCID 10457 | — |
| 용매 | Acetic Anhydride | HCID 7918 | — |
| 생성물 | Oxonane-2,9-dione | HCID 9543534 | 50.4% |
반응 단계
A solution of suberic acid (5.0 g, 28.7 mmol) in acetic anhydride (10 mL) was heated at reflux for 1 h. After cooling to RT, the solvent was removed in vacuo. The pale yellow residue was recrystallized from acetonitrile. After filtration and drying to the vacuum pump, the oxonane-2,9-dione was obtained as a white solid (2.26 g, 50.4% yield).
출처 및 근거
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| 특허 번호 | US07923579B2 |
| 출처 데이터셋 | uspto-grants-2011_04 |
| ORD ID | ord-de2bb5712e94419a90ec52684ee6e963 |
| 출처 메모 | uspto-grants-2011_04 |