HuagongsheHuagongshe Chemistry Print Report · For research reference only
N-[(3-Bromophenyl)methyl]methanesulfonamide → HCID 86617419, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | N-[(3-Bromophenyl)methyl]methanesulfonamide | HCID 6464358 | — |
| Reactant | Tert-butyl 2-hydroxy-6-{[4-(4,4,5,5-tetramethyl-1,3,2-dioxaborolan-2-yl)phenoxy]methyl}-3-(trifluoromethyl)benzoate | HCID 67119153 | — |
| Product | HCID 86617419 | HCID 86617419 | — |
Reaction Steps
According to a method similar to Example (31), from N-(3-bromobenzyl)methanesulfonamide (119 mg, 0.45 mmol) and tert-butyl 2-hydroxy-6-{[4-(4,4,5,5-tetramethyl-1,3,2-dioxaborolan-2-yl)phenoxy]methyl}-3-(trifluoromethyl)benzoate (250 mg, 0.51 mmol) obtained in Example (22-4), the title compound was obtained as a pale brown powder (49 mg, yield: 20%).
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US07923573B2 |
| Source dataset | uspto-grants-2011_04 |
| ORD ID | ord-d9182f3deb13444e9d3c31272fc8613d |
| Source note | uspto-grants-2011_04 |