HuagongsheHuagongshe Chemistry Print Report · For research reference only
Tert-butyl 6-(bromomethyl)-2-[(tert-butoxycarbonyl)oxy]-3-(trifluoromethyl)benzoate → HCID 67119110, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Tert-butyl 6-(bromomethyl)-2-[(tert-butoxycarbonyl)oxy]-3-(trifluoromethyl)benzoate | HCID 67119234 | — |
| Reactant | HCID 86761300 | HCID 86761300 | — |
| Product | HCID 67119110 | HCID 67119110 | — |
Reaction Steps
According to a method similar to Example (40-2), Example (33-5) and Example (17-4), from tert-butyl 6-(bromomethyl)-2-[(tert-butoxycarbonyl)oxy]-3-(trifluoromethyl)benzoate (137 mg, 0.325 mmol) obtained in Example (28-5) and methyl [4′-hydroxy-2-(1-hydroxyethyl)-1,1′-biphenyl-4-yl]acetate (93 mg, 0.325 mmol) obtained in Example (88-1), the title compound was obtained as a pale yellow oil (60 mg, yield: 34%).
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US07923573B2 |
| Source dataset | uspto-grants-2011_04 |
| ORD ID | ord-fd67cb86807b4c77b71e4f8887c50e9e |
| Source note | uspto-grants-2011_04 |