HuagongsheHuagongshe Chemistry Print Report · For research reference only
Tert-butyl 6-(bromomethyl)-2-[(tert-butoxycarbonyl)oxy]-3-(trifluoromethyl)benzoate → HCID 67119365, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Tert-butyl 6-(bromomethyl)-2-[(tert-butoxycarbonyl)oxy]-3-(trifluoromethyl)benzoate | HCID 67119234 | — |
| Reactant | HCID 67119269 | HCID 67119269 | — |
| Product | HCID 67119365 | HCID 67119365 | — |
Reaction Steps
According to a method similar to Example (40-2), Example (33-5) and Example (17-4), from methyl 2-(2,3-difluoro-4′-hydroxy-1,1′-biphenyl-4-yl)propanoate (193 mg, 0.661 mmol) and tert-butyl 6-(bromomethyl)-2-[(tert-butoxycarbonyl)oxy]-3-(trifluoromethyl)benzoate (306 mg, 0.726 mmol) obtained in Example (28-5), the title compound was obtained as a white powder (45 mg, yield: 12%).
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US07923573B2 |
| Source dataset | uspto-grants-2011_04 |
| ORD ID | ord-fd99ab9fb39a404ab0e6988b5e50ca05 |
| Source note | uspto-grants-2011_04 |