HuagongsheHuagongshe Chemistry Print Report · For research reference only
Carbamazepine → HCID 67107456, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Carbamazepine | HCID 2554 | — |
| Reactant | 2,6-Pyridinedicarboxylic acid | HCID 10367 | — |
| Solvent | Ethanol | HCID 702 | — |
| Product | HCID 67107456 | HCID 67107456 | — |
Reaction Steps
36 mg (0.1524 mmol) carbamazepine and 26 mg (0.1556 mmol) 2,6-pyridinedicarboxylic acid were dissolved in approximately 2 mL ethanol. Slow evaporation of the solvent yielded clear needles of a 1:1 carbamazepine/2,6-pyridinedicarboxylic acid co-crystal, as shown in FIG. 54A-B.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US07927613B2 |
| Source dataset | uspto-grants-2011_04 |
| ORD ID | ord-69fc570bbe844cc3b8190e9f7c9ca3de |
| Source note | uspto-grants-2011_04 |