HuagongsheHuagongshe Chemistry Print Report · For research reference only
Ethanol → HCID 67107880, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Ethanol | HCID 702 | — |
| Reactant | Carbamazepine | HCID 2554 | — |
| Reactant | 5-Nitroisophthalic acid | HCID 12069 | — |
| Solvent | Methanol | HCID 887 | — |
| Product | HCID 67107880 | HCID 67107880 | — |
Reaction Steps
40 mg (0.1693 mmol) carbamazepine and 30 mg (0.1421 mmol) 5-nitroisophthalic acid were dissolved in approximately 3 mL methanol or ethanol. Slow evaporation of the solvent yielded yellow needles of a 1:1 carbamazepine/5-nitroisophthalic acid co-crystal, as shown in FIG. 55A-B.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US07927613B2 |
| Source dataset | uspto-grants-2011_04 |
| ORD ID | ord-664a081a31954368a8196399dc1d5b5d |
| Source note | uspto-grants-2011_04 |