HuagongsheHuagongshe Chemistry Print Report · For research reference only
Ethanol → HCID 67547676, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Ethanol | HCID 702 | — |
| Reactant | Carbamazepine | HCID 2554 | — |
| Reactant | 1,3,5,7-Adamantanetetracarboxylic acid | HCID 622495 | — |
| Solvent | Methanol | HCID 887 | — |
| Product | HCID 67547676 | HCID 67547676 | — |
Reaction Steps
15 mg (0.1524 mmol) carbamazepine and 20 mg (0.1556 mmol) 1,3,5,7-adamantanetetracarboxylic acid were dissolved in approximately 1 mL methanol or 1 mL ethanol. Slow evaporation of the solvent yields clear plates of a 2:1 carbamazepine/1,3,5,7-adamantanetetracarboxylic acid co-crystal, as shown in FIG. 56A-B.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US07927613B2 |
| Source dataset | uspto-grants-2011_04 |
| ORD ID | ord-4a4a81456b774528a6f5692e987eca0f |
| Source note | uspto-grants-2011_04 |