HuagongsheHuagongshe Chemistry Print Report · For research reference only
Carbamazepine → HCID 67108016, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Carbamazepine | HCID 2554 | — |
| Reactant | Quinone | HCID 4650 | — |
| Reactant | Tetrahydrofuran | HCID 8028 | — |
| Solvent | Methanol | HCID 887 | — |
| Product | HCID 67108016 | HCID 67108016 | — |
Reaction Steps
25 mg (0.1058 mmol) carbamazepine and 11 mg (0.1018 mmol) benzoquinone was dissolved in 2 mL methanol or THF. Slow evaporation of the solvent produced an average yield of yellow crystals of a 1:1 carbamazepine/benzoquinone co-crystal, as shown in FIG. 57A-B.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US07927613B2 |
| Source dataset | uspto-grants-2011_04 |
| ORD ID | ord-33dffa4888f8422f9546f53a90b4a3a0 |
| Source note | uspto-grants-2011_04 |