HuagongsheHuagongshe Chemistry Print Report · For research reference only
Carbamazepine → HCID 131728783, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Carbamazepine | HCID 2554 | — |
| Reactant | 1,3,5-Benzenetricarboxylic acid | HCID 11138 | — |
| Solvent | Methanol | HCID 887 | — |
| Solvent | Dichloromethane | HCID 6344 | — |
| Product | HCID 131728783 | HCID 131728783 | — |
Reaction Steps
36 mg (0.1524 mmol) carbamazepine and 31 mg (0.1475 mmol) trimesic acid were dissolved in a solvent mixture of approximately 2 mL methanol and 2 mL dichloromethane. Slow evaporation of the solvent mixture yielded white starbursts of a 1:1 carbamazepine/trimesic acid co-crystal, as shown in FIG. 58A-B.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US07927613B2 |
| Source dataset | uspto-grants-2011_04 |
| ORD ID | ord-6416a4aeec8943aabd6bb6df8014258e |
| Source note | uspto-grants-2011_04 |